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Synthesis and application of bilayer-surfactant-enveloped Fe3O4 nanoparticles: water-based bilayer-surfactant-enveloped ferrofluids
Chen, Bai-yi1; Qiu, Jian-hui1; Feng, Hui-xia2
刊名INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS
2016-02
卷号23期号:2页码:234-240
关键词magnetic fluids iron oxides nanoparticles bilayers sodium oleate polyethylene glycol
ISSN号1674-4799
DOI10.1007/s12613-016-1231-2
英文摘要Superparamagnetic carbon-coated Fe3O4 nanoparticles with high magnetization (85 emu center dot g(-1)) and high crystallinity were synthesized using polyethylene glycol-4000 (PEG (4000)) as a carbon source. Fe3O4 water-based bilayer-surfactant-enveloped ferrofluids were subsequently prepared using sodium oleate and PEG (4000) as dispersants. Analyses using X-ray photoelectron spectroscopy, X-ray diffraction, and Fourier-transform infrared spectroscopy indicate that the Fe3O4 nanoparticles with a bilayer surfactant coating retain the inverse spinel-type structure and are successfully coated with sodium oleate and PEG (4000). Transmission electron microscopy, vibrating sample magnetometry, and particle-size analysis results indicate that the coated Fe3O4 nanoparticles also retain the good saturation magnetization of Fe3O4 (79.6 emu center dot g(-1)) and that the particle size of the bilayer-surfactant-enveloped Fe3O4 nanoparticles is 42.97 nm, which is substantially smaller than that of the unmodified Fe3O4 nanoparticles (486.2 nm). UV-vis and zeta-potential analyses reveal that the ferrofluids does not agglomerate for 120 h at a concentration of 4 g center dot L-1, which indicates that the ferrofluids are highly stable.
资助项目Fundamental Research Funds for the Universities of Gansu[1105ZTC136]
WOS研究方向Materials Science ; Metallurgy & Metallurgical Engineering ; Mining & Mineral Processing
语种英语
出版者SPRINGER
WOS记录号WOS:000369238200014
状态已发表
内容类型期刊论文
源URL[http://119.78.100.223/handle/2XXMBERH/33787]  
专题石油化工学院
教务处(创新创业学院)
通讯作者Qiu, Jian-hui; Feng, Hui-xia
作者单位1.Akita Prefectural Univ, Fac Syst Engn, Dept Machine Intelligence & Syst Engn, Akita 0150055, Japan
2.Lanzhou Univ Technol, Coll Petrochem Technol, Lanzhou 730050, Peoples R China
推荐引用方式
GB/T 7714
Chen, Bai-yi,Qiu, Jian-hui,Feng, Hui-xia. Synthesis and application of bilayer-surfactant-enveloped Fe3O4 nanoparticles: water-based bilayer-surfactant-enveloped ferrofluids[J]. INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS,2016,23(2):234-240.
APA Chen, Bai-yi,Qiu, Jian-hui,&Feng, Hui-xia.(2016).Synthesis and application of bilayer-surfactant-enveloped Fe3O4 nanoparticles: water-based bilayer-surfactant-enveloped ferrofluids.INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS,23(2),234-240.
MLA Chen, Bai-yi,et al."Synthesis and application of bilayer-surfactant-enveloped Fe3O4 nanoparticles: water-based bilayer-surfactant-enveloped ferrofluids".INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS 23.2(2016):234-240.
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