The Preparation of Size-controlled Antimony Nanoparticles by Electrochemical Method

doi:10.4028/www.scientific.net/KEM.562-565.716

	The Preparation of Size-controlled Antimony Nanoparticles by Electrochemical Method
	Xu, Jianlin 2,3; Wang, Jia 2,3; Zhang, Lihui 1; Niu, Lei 3; Zhang, Jianbin 2,3; Ran, Fen 2,3; Yan, Xiaobin 2,3
	2013
关键词	Antimony Nanoparticles Electrochemical Method
卷号	562-565
DOI	10.4028/www.scientific.net/KEM.562-565.716
页码	716-+
英文摘要	This paper prepared some antimony nanoparticles with different particle size by electrochemical method. A method of preparing size-controlled antimony nanoparticles was established in the hydrochloric acid solution, which alkyphenol ethoxylates emulsifier was used as surface dispersants by electrochemical technology based on the optimization of the preparation technology. Those obtained antimony nanoparticles was characterized and analyzed by means of transmission electron microscopy (TEM), Fourier transform infrared absorption spectrum (FT-IR), X-ray diffraction (XRD). The experiment results show that alkyphenol ethoxylates emulsifier can effectively coat on the surface of antimony nanoparticles, current density and electrolysis time have an important influence on the particle size of those obtained antimony nanoparticles. When the current density is 25mA/cm(2) and electrolysis time is 30minutes, spherical antimony nanoparticles with an average diameter of 12nm and good dispersion can be prepared.
会议录	MICRO-NANO TECHNOLOGY XIV, PTS 1-4
会议录出版者	TRANS TECH PUBLICATIONS LTD
会议录出版地	KREUZSTRASSE 10, 8635 DURNTEN-ZURICH, SWITZERLAND
语种	英语
资助项目	Natural Science Foundation of Zhejiang Province of China[LY12E01002] ; Open Fund of State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials[SKL12012]
WOS研究方向	Science & Technology - Other Topics ; Materials Science
WOS记录号	WOS:000324503700130
内容类型	会议论文
源URL	[http://119.78.100.223/handle/2XXMBERH/37022]
专题	材料科学与工程学院新能源学院省部共建有色金属先进加工与再利用国家重点实验室
通讯作者	Xu, Jianlin
作者单位	1.Avic Xian Aero Engine Grp LTD, Res & Dev Ctr, Xian 710000, Peoples R China 2.Lanzhou Univ Technol, Wenzhou Res Inst Pump & Valve Engn, Wenzhou 325000, Peoples R China 3.Lanzhou Univ Technol, State Key Lab Gansu Adv Nonferrous Met Mat, Lanzhou 730050, Peoples R China
推荐引用方式 GB/T 7714	Xu, Jianlin,Wang, Jia,Zhang, Lihui,et al. The Preparation of Size-controlled Antimony Nanoparticles by Electrochemical Method[C]. 见:.