Synthesis of Different-Sized La0.7Sr0.3MnO3 Nanoparticles via a Polyacrylamide Gel Route and Their Magnetocaloric Properties
Wang, Y. F.1,2; Yang, H.1,2
刊名JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM
2013-12
卷号26期号:12页码:3463-3467
关键词La0.7Sr0.3MnO3 Nanoparticles Polyacrylamide gel route Chelating agents Magnetocaloric effect
ISSN号1557-1939
DOI10.1007/s10948-013-2190-8
英文摘要In this work, a polyacrylamide gel route was used to synthesize La0.7Sr0.3MnO3 nanoparticles. It is shown that single-phase La0.7Sr0.3MnO3 nanoparticles with a rhombohedral perovskite structure can be prepared at a calcination temperature of 600 A degrees C when separately using citric acid, tartaric acid, acetic acid, oxalic acid, and EDTA as the chelating agent. The particles prepared using the five chelating agents are nearly spherical in shape with a narrow diameter distribution, and have an average size of 24, 28, 36, 38, and 50 nm, respectively. Magnetic properties of the 24 and 50 nm samples (termed as samples S1 and S5, respectively) were investigated. It is revealed that the samples have a similar ferromagnetic Curie temperature T (C) , and exhibit a typical second-order magnetic phase transition near T (C) . The maximum magnetic entropy change at an applied magnetic field of 15 kOe is obtained to be about 0.71 and 0.74 J kg(-1) K-1 for the 24 and 50 nm samples, respectively.
资助项目National Natural Science Foundation of China[50962009][51262018] ; Hongliu Outstanding Talents Foundation of Lanzhou University of Technology[J201205]
WOS研究方向Physics
语种英语
出版者SPRINGER
WOS记录号WOS:000325949200017
状态已发表
内容类型期刊论文
源URL[http://119.78.100.223/handle/2XXMBERH/34567]  
专题省部共建有色金属先进加工与再利用国家重点实验室
材料科学与工程学院
理学院
通讯作者Yang, H.
作者单位1.Lanzhou Univ Technol, State Key Lab Gansu Adv Nonferrous Met Mat, Lanzhou 730050, Peoples R China
2.Lanzhou Univ Technol, Sch Sci, Lanzhou 730050, Peoples R China
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GB/T 7714
Wang, Y. F.,Yang, H.. Synthesis of Different-Sized La0.7Sr0.3MnO3 Nanoparticles via a Polyacrylamide Gel Route and Their Magnetocaloric Properties[J]. JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM,2013,26(12):3463-3467.
APA Wang, Y. F.,&Yang, H..(2013).Synthesis of Different-Sized La0.7Sr0.3MnO3 Nanoparticles via a Polyacrylamide Gel Route and Their Magnetocaloric Properties.JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM,26(12),3463-3467.
MLA Wang, Y. F.,et al."Synthesis of Different-Sized La0.7Sr0.3MnO3 Nanoparticles via a Polyacrylamide Gel Route and Their Magnetocaloric Properties".JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM 26.12(2013):3463-3467.
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