Submicron LaB6 powders with high purity prepared in large scale by salt-assisted combustion synthesis
Li, Zhengning; Ou, Yujing; La, Peiqing; Shi, Yu
刊名JOURNAL OF RARE EARTHS
2018-06
卷号36期号:6页码:623-629
关键词Combustion synthesis LaB6 powders Purity Particle size Rare earths
ISSN号1002-0721
DOI10.1016/j.jre.2018.01.003
英文摘要LaB6 powders were synthesized in large scale by salt-assisted combustion synthesis (CS) with different NaCl diluent contents. The variety of phases, particle size and purity of the powders were investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), and transmission electron microscope (TEM). With increase of NaCl content, the adiabatic combustion temperature of the reaction system linearly declines, the average particle size of leached products decreases, the impurity phases are easier to remove, and the products purity enhances obviously. When NaCl content is 40 wt%, the purity of the superfine powders of LaB6 is more than 98 wt%, and the average particle size is 380 nm. (C) 2018 Chinese Society of Rare Earths. Published by Elsevier B.V. All rights reserved.
资助项目National Natural Science Foundation of China[51561020]
WOS研究方向Chemistry
语种英语
出版者ELSEVIER SCIENCE BV
WOS记录号WOS:000434782300009
状态已发表
内容类型期刊论文
源URL[http://119.78.100.223/handle/2XXMBERH/32609]  
专题省部共建有色金属先进加工与再利用国家重点实验室
材料科学与工程学院
石油化工学院
通讯作者La, Peiqing
作者单位Lanzhou Univ Technol, State Key Lab Adv Proc & Recycling Nonferrous Met, Lanzhou 730050, Gansu, Peoples R China
推荐引用方式
GB/T 7714
Li, Zhengning,Ou, Yujing,La, Peiqing,et al. Submicron LaB6 powders with high purity prepared in large scale by salt-assisted combustion synthesis[J]. JOURNAL OF RARE EARTHS,2018,36(6):623-629.
APA Li, Zhengning,Ou, Yujing,La, Peiqing,&Shi, Yu.(2018).Submicron LaB6 powders with high purity prepared in large scale by salt-assisted combustion synthesis.JOURNAL OF RARE EARTHS,36(6),623-629.
MLA Li, Zhengning,et al."Submicron LaB6 powders with high purity prepared in large scale by salt-assisted combustion synthesis".JOURNAL OF RARE EARTHS 36.6(2018):623-629.
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