High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures
Shen, Sijia3; Li, Hongbo3; Yang, Lingwei2; Li N(李娜)1; Wu, Jinting3; Zhao, Tingxing3
刊名POLYMER TESTING
2022-03-01
卷号107页码:8
关键词Polyimide Nanoindentation Interface Micro-mechanics High temperature mechanics
ISSN号0142-9418
DOI10.1016/j.polymertesting.2022.107483
通讯作者Li, Hongbo(li-honggg@163.com) ; Yang, Lingwei(lingwei.yang@cardc.cn)
英文摘要In this work, a novel high-throughput methodology based on combinations of nanoindentation, indentation creep and push-in methods, is proposed to measure in-situ the micro-mechanical properties of typical polymer matrix composites at a wide temperature range. The Young's modulus and strain rate sensitivity of a polyimide matrix and the interfacial shear strength in a quartz fiber reinforced polyimide matrix composite are measured at 25-350 degrees C for the first time. The results highlight a linear softening of the polyimide matrix at high temperatures, which is evidenced by the approximate linear decrease of Young's modulus from approximate to 5.0 GPa at 25 degrees C to approximate to 1.1 GPa at 350 degrees C. In comparison, the strain rate sensitivity of the polyimide matrix is increased, from approximate to 0.032 at 25 degrees C to approximate to 0.062 at 350 degrees C. This evidences a stronger visco-plasticity of polyimide at higher temperatures. The shear strength of the fiber/matrix interface is also temperature dependent. As the testing temperature increases from 25 to 300 degrees C, the shear strength is decreased from approximate to 147 MPa to approximate to 40 MPa. Specially, the interfacial strength is extremely low at 350 degrees C (approximate to 4 MPa), evidencing a failure of the composite at this temperature.
分类号一类
资助项目National Natural Science Foundation of China[11902333]
WOS关键词STRAIN-RATE SENSITIVITY ; SHEAR-STRENGTH ; PUSH-IN ; NANOINDENTATION ; BEHAVIOR ; TESTS
WOS研究方向Materials Science ; Polymer Science
语种英语
WOS记录号WOS:000765380600009
资助机构National Natural Science Foundation of China
其他责任者Li, Hongbo ; Yang, Lingwei
内容类型期刊论文
源URL[http://dspace.imech.ac.cn/handle/311007/88766]  
专题力学研究所_非线性力学国家重点实验室
作者单位1.Chinese Acad Sci, Inst Mech, LNM, Beijing 100190, Peoples R China
2.China Aerodynam Res & Dev Ctr, Hyperveloc Aerodynam Inst, Mianyang 621000, Sichuan, Peoples R China;
3.Southwest Univ Sci & Technol, Sch Mat Sci & Engn, Mianyang 621000, Sichuan, Peoples R China;
推荐引用方式
GB/T 7714
Shen, Sijia,Li, Hongbo,Yang, Lingwei,et al. High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures[J]. POLYMER TESTING,2022,107:8.
APA Shen, Sijia,Li, Hongbo,Yang, Lingwei,李娜,Wu, Jinting,&Zhao, Tingxing.(2022).High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures.POLYMER TESTING,107,8.
MLA Shen, Sijia,et al."High-throughput screening the micro-mechanical properties of polyimide matrix composites at elevated temperatures".POLYMER TESTING 107(2022):8.
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