Ultrasensitive Determination of Tetrabromobisphenol A by Covalent Organic Framework Based Solid Phase Microextraction Coupled with Constant Flow Desorption Ionization Mass Spectrometry
Gao, Wei; Tian, Yong; Liu, Huan; Cai, Yaqi; Liu, Aifeng; Yu, Yong-Liang; Zhao, Zongshan; Jiang, Guibin
刊名ANALYTICAL CHEMISTRY
2019
卷号91期号:1页码:772-775
ISSN号0003-2700
英文摘要Rapid detection of ultratrace pollutants in complex matrixes is a great challenge for studying their environmental behaviors and impacts. In this work, a method is developed by combining covalent organic framework (COF) based solid phase microextraction (SPME) with constant flow desorption ionization mass spectrometry for rapid detection of trace tetrabromobisphenol A (TBBPA) in multiple water media. The limits of detection and qualification are 0.92 and 3.1 ng L-1 for TBBPA, respectively. The linear range is between 0.01 and 10 mu g L-1 (R-2 = 0.9992), and the relative standard deviations with single fiber and multiple fibers are 6.4% and 6.7% (0.1 mu g L-1, n = 9), respectively. The detection of nanogram per liter levels of TBBPA in tap water, river water, seawater, and beverage can be achieved in 7 min.
内容类型期刊论文
源URL[http://ir.rcees.ac.cn/handle/311016/43049]  
专题生态环境研究中心_环境化学与生态毒理学国家重点实验室
作者单位1.Northeastern Univ, Dept Chem, Coll Sci, Res Ctr Analyt Sci, Box 332, Shenyang 110819, Liaoning, Peoples R China
2.Chinese Acad Sci, Qingdao Inst Bioenergy & Bioproc Technol, CAS Key Lab Biobased Mat, Qingdao 266101, Peoples R China
3.Chinese Acad Sci, Res Ctr Ecoenvironm Sci, State Key Lab Environm Chem & Ecotoxicol, Beijing 100085, Peoples R China
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Gao, Wei,Tian, Yong,Liu, Huan,et al. Ultrasensitive Determination of Tetrabromobisphenol A by Covalent Organic Framework Based Solid Phase Microextraction Coupled with Constant Flow Desorption Ionization Mass Spectrometry[J]. ANALYTICAL CHEMISTRY,2019,91(1):772-775.
APA Gao, Wei.,Tian, Yong.,Liu, Huan.,Cai, Yaqi.,Liu, Aifeng.,...&Jiang, Guibin.(2019).Ultrasensitive Determination of Tetrabromobisphenol A by Covalent Organic Framework Based Solid Phase Microextraction Coupled with Constant Flow Desorption Ionization Mass Spectrometry.ANALYTICAL CHEMISTRY,91(1),772-775.
MLA Gao, Wei,et al."Ultrasensitive Determination of Tetrabromobisphenol A by Covalent Organic Framework Based Solid Phase Microextraction Coupled with Constant Flow Desorption Ionization Mass Spectrometry".ANALYTICAL CHEMISTRY 91.1(2019):772-775.
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