Determination of organotin compounds by liquid chromatography coupled with inductively coupled plasma mass spectrometric detection

	Determination of organotin compounds by liquid chromatography coupled with inductively coupled plasma mass spectrometric detection
	Miao, Jing 1,2; Yu Zhen-Hua 2; Wang Xiao-Ru 2; Lee, Frank S. C.2; Chen Dengyu 2
刊名	CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
	2008-02
卷号	36 期号:2 页码:235-237
关键词	organotin liquid chromatography inductively coupled plasma mass spectrometry seawater
ISSN号	0253-3820
英文摘要	A high performance liquid chromatography-inductively coupled plasma mass spectrometric (HPLC-ICP-MS) method were developed for the analysis of organotin compounds in seawater. The data presented show that, dibutyltin (DBT), monobutyltin (MBT), tributyltin (TBT) and triphenyltin (TPhT) were detected by two different C-18 stationary phase material with decreased particle by the buffer solution of V(acetonitrile) : V(H2O): V(acetic acid): V(TEA) = 65:23:12:0.005%, the flow rate is 0.2 mL/min of C-18-AES column and 0.4 mL/min of TC-C-18 column, baseline resolution of DBT, MBT, TBT and TPhT can be achieved with TC-C-18 column. The detection limits was 30 ng/L for DBT, 50 ng/L for MBT, 80 ng/L for TBT and 10 ng/L for TPhT. The concentration of DBT, TPhT in Qindao seawater used in this experiment were 35 ng/L, 20 ng/L respectively.
WOS研究方向	Chemistry
语种	中文
出版者	ELSEVIER SCIENCE INC
WOS记录号	WOS:000254252200021
内容类型	期刊论文
源URL	[http://ir.fio.com.cn:8080/handle/2SI8HI0U/26675]
专题	自然资源部第一海洋研究所
通讯作者	Miao, Jing
作者单位	1.Ocean Univ, Dept Chem, Qingdao 266006, Peoples R China 2.State Ocean Adm, Inst Oceanog 1, Qingdao 266061, Peoples R China
推荐引用方式 GB/T 7714	Miao, Jing,Yu Zhen-Hua,Wang Xiao-Ru,et al. Determination of organotin compounds by liquid chromatography coupled with inductively coupled plasma mass spectrometric detection[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2008,36(2):235-237.
APA	Miao, Jing,Yu Zhen-Hua,Wang Xiao-Ru,Lee, Frank S. C.,&Chen Dengyu.(2008).Determination of organotin compounds by liquid chromatography coupled with inductively coupled plasma mass spectrometric detection.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,36(2),235-237.
MLA	Miao, Jing,et al."Determination of organotin compounds by liquid chromatography coupled with inductively coupled plasma mass spectrometric detection".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 36.2(2008):235-237.