One-step Extraction and Sensitive Measurement of Polar and Non-Polar Pollutants Simultaneously in Soil Using Modified Ultrasonic Technology with in situ Derivatization

CORC > 中国地质调查局 > 中国地质调查局 > 中国地质科学院水文地质环境地质研究所

	One-step Extraction and Sensitive Measurement of Polar and Non-Polar Pollutants Simultaneously in Soil Using Modified Ultrasonic Technology with in situ Derivatization
	Gui, Jianye 2; Zhang, Chenling ; Zhang, Yongtao ; Zhang, Li ; Qi, Jixiang ; Li, Xiaoya ; Tai, Laisheng ; Zhao, Guoxing
刊名	ASIAN JOURNAL OF CHEMISTRY
	2014
卷号	26 期号:9 页码:2624-2628
关键词	Ultrasonic extraction Herbicide Phenols Organochlorine Polar Non-polar NCI Soil
ISSN号	0970-7077
英文摘要	A simple low-cost ultrasonic extraction procedure has been developed for determination of polar aromatic acids, polar phenols and nonpolar pesticides simultaneously in soil. This procedure was accomplished by in situ derivatization as well as elevated temperature, increased power and dispersing intimate contact of solvent with samples. Combined with GC/NCI/MS method, the sensitivity was improved remarkably because of the enhanced electronegativity of derivatized products of herbicide and phenols as well as the intrinsic electronegativity of organochlorine. The method presented here showed that the modified ultrasonic extraction method can be a robust preparation methodology for both polar and nonpolar organic contaminants which can be applied to solid sample pre-treatment extensively.
学科主题	岩矿鉴定与测试
WOS关键词	PRESSURIZED FLUID EXTRACTION ; PESTICIDES ; HERBICIDES
WOS研究方向	Chemistry
语种	英语
出版者	ASIAN JOURNAL OF CHEMISTRY
WOS记录号	WOS:000335841000027
内容类型	期刊论文
源URL	[http://119.78.100.197/handle/2HKVOGP0/40372]
专题	中国地质科学院水文地质环境地质研究所
作者单位	1.CAGS, Inst Hydrogeol & Environm Geol, Zhengding 050803, Peoples R China 2.中国地质科学院水文地质环境地质研究所
推荐引用方式 GB/T 7714	Gui, Jianye,Zhang, Chenling,Zhang, Yongtao,et al. One-step Extraction and Sensitive Measurement of Polar and Non-Polar Pollutants Simultaneously in Soil Using Modified Ultrasonic Technology with in situ Derivatization[J]. ASIAN JOURNAL OF CHEMISTRY,2014,26(9):2624-2628.
APA	Gui, Jianye.,Zhang, Chenling.,Zhang, Yongtao.,Zhang, Li.,Qi, Jixiang.,...&Zhao, Guoxing.(2014).One-step Extraction and Sensitive Measurement of Polar and Non-Polar Pollutants Simultaneously in Soil Using Modified Ultrasonic Technology with in situ Derivatization.ASIAN JOURNAL OF CHEMISTRY,26(9),2624-2628.
MLA	Gui, Jianye,et al."One-step Extraction and Sensitive Measurement of Polar and Non-Polar Pollutants Simultaneously in Soil Using Modified Ultrasonic Technology with in situ Derivatization".ASIAN JOURNAL OF CHEMISTRY 26.9(2014):2624-2628.