Preparation of ZnO Nanostructures by Thermal Degradation of Zinc Alginate Fibers | |
Kong Qing-Shan1,2; Wu Xing-Long3; Guo Yu-Guo3; Wang Yi-Qian1; Xia Yan-Zhi1; Yu Jian2; Liu Hai-Hua4; Duan Xiao-Feng4 | |
刊名 | ACTA PHYSICO-CHIMICA SINICA |
2008-12-01 | |
卷号 | 24期号:12页码:2179-2184 |
关键词 | Zinc Alginate Fiber Zno Nanorod Thermal Degradation |
ISSN号 | 1000-6818 |
DOI | 10.3866/PKU.WHXB20081206 |
英文摘要 | Zinc alginate (Alg-Zn) fibers were obtained by wet spinning of sodium alginate (Alg-Na) into a coagulating bath containing an aqueous zinc chloride solution. ZnO nanostructures were prepared by thermal degradation of the as-obtained zinc alginate fibers at different temperatures in air. The compositions, morphologies, and microstructures of products were investigated by thermal gravimetry (TG), X-ray diffraction (XRD), electron energy-loss spectroscopy (EELS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). Annealing time and temperature influenced Final structures and shapes of ZnO nanostructures. ZnO nanorods with diameters of about 120 nm were obtained at 800 degrees C and with a reaction time of more than 24. It in air. A ZnO growth mechanism was proposed by a careful investigation of ZnO nanostructures after different thermal treatment times. |
语种 | 英语 |
出版者 | PEKING UNIV PRESS |
WOS记录号 | WOS:000262024900006 |
内容类型 | 期刊论文 |
源URL | [http://ir.iccas.ac.cn/handle/121111/64005] |
专题 | 中国科学院化学研究所 |
通讯作者 | Xia Yan-Zhi |
作者单位 | 1.Qingdao Univ, Adv Fibers & Modern Text Cultivat Base State Key, Qingdao 266071, Shandong, Peoples R China 2.Tsinghua Univ, Dept Chem Engn, Inst Polymer Sci & Technol, Beijing 100084, Peoples R China 3.Chinese Acad Sci, Inst Chem, Beijing 100190, Peoples R China 4.Chinese Acad Sci, Inst Phys, Beijing Lab Electron Microscopy, Beijing 100190, Peoples R China |
推荐引用方式 GB/T 7714 | Kong Qing-Shan,Wu Xing-Long,Guo Yu-Guo,et al. Preparation of ZnO Nanostructures by Thermal Degradation of Zinc Alginate Fibers[J]. ACTA PHYSICO-CHIMICA SINICA,2008,24(12):2179-2184. |
APA | Kong Qing-Shan.,Wu Xing-Long.,Guo Yu-Guo.,Wang Yi-Qian.,Xia Yan-Zhi.,...&Duan Xiao-Feng.(2008).Preparation of ZnO Nanostructures by Thermal Degradation of Zinc Alginate Fibers.ACTA PHYSICO-CHIMICA SINICA,24(12),2179-2184. |
MLA | Kong Qing-Shan,et al."Preparation of ZnO Nanostructures by Thermal Degradation of Zinc Alginate Fibers".ACTA PHYSICO-CHIMICA SINICA 24.12(2008):2179-2184. |
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