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Preparation of aligned carbon nanotube arrays by pyrolysis of iron(II) phthalocyanine and ethylene
Peng Ai-Ping1,2; Zhang Hao3; Wang Zhi-Yong2; Shi Zu-Jin2; Gu Zhen-Nan2; Cao Gao-Ping3; Gao Li-Jun1
刊名CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
2007-12-10
卷号28期号:12页码:2229-2233
关键词Aligned Carbon Nanotube Array Iron(Ii) Phthalocyanine Thermal Chemical Vapor Deposition
ISSN号0251-0790
英文摘要Aligned carbon nanotube arrays (ACNTA) with 210 mu m in length were prepared by pyrolysis of iron(H) phthalocyanine(FePc) and ethylene(C2H4). The as-grown ACNTA, which were well-aligned and pure, were characterized by scanning electron microscopy (SEM), transmission electron microscopy(TEM), Raman spectrum and X-ray photoelectron spectroscopy (XPS). The influence of experimental conditions, such as temperature, growth time, and flow rate of C2H4 on the formation of ACNTA were systematically investigated. The results indicate that 800 degrees C was the most suitable temperature for the preparation of long ACNTA by pyrolysis of FePc and C2H4, the activity of catalyst could be kept for a rather long time(60 min), the addition of C2H4 significantly enhanced the growth speed of ACNTA and 50 cm(3)/min was found to be the optimal flow rate for the formation of ACNTA.
语种英语
出版者HIGHER EDUCATION PRESS
WOS记录号WOS:000251953400001
内容类型期刊论文
源URL[http://ir.iccas.ac.cn/handle/121111/62037]  
专题中国科学院化学研究所
通讯作者Gao Li-Jun
作者单位1.Nanchang Univ, Dept Chem, Nanchang 330031, Peoples R China
2.Peking Univ, Coll Chem & Mol Engn, State Key Lab Rare Earth Mat Chem & Applicat, Beijing Natl Lab Mol Sci, Beijing 100871, Peoples R China
3.Res Inst Chem Def, Beijing 100083, Peoples R China
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GB/T 7714
Peng Ai-Ping,Zhang Hao,Wang Zhi-Yong,et al. Preparation of aligned carbon nanotube arrays by pyrolysis of iron(II) phthalocyanine and ethylene[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2007,28(12):2229-2233.
APA Peng Ai-Ping.,Zhang Hao.,Wang Zhi-Yong.,Shi Zu-Jin.,Gu Zhen-Nan.,...&Gao Li-Jun.(2007).Preparation of aligned carbon nanotube arrays by pyrolysis of iron(II) phthalocyanine and ethylene.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,28(12),2229-2233.
MLA Peng Ai-Ping,et al."Preparation of aligned carbon nanotube arrays by pyrolysis of iron(II) phthalocyanine and ethylene".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 28.12(2007):2229-2233.
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