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Controlled synthesis of ammonium manganese tri-fluoride nanoparticles with enhanced electrochemical performance
Khan, Jamshid1; Ullah, Hameed1,2; Sajjad, Muhammad3; Jatoi, Wahid Bux4; Ali, Akbar5,6; Khan, Karim7,8; Thebo, Khalid Hussain6
刊名MATERIALS RESEARCH EXPRESS
2019-07-01
卷号6期号:7页码:11
关键词metal fluorides nanoparticles electrochemical voltammetry performance
ISSN号2053-1591
DOI10.1088/2053-1591/ab18bb
英文摘要Herein, ammonium manganese tri-fluoride (NH4MnF3) nanoparticles (similar to 20-80 nm) were synthesized via easy, non-sophisticated and environment friendly reverse micro-emulsion method for the first time. Two type i.e. sintered and non-sintered NH4MnF3 nanoparticles were prepared with different ratio by changing water to surfactant percentage while keeping the temperature constant at 22 degrees C. The structural, morphological and optical properties of as-prepared nanoparticles were investigated by x-ray diffraction (XRD), energy-dispersive x-ray spectroscopy (EDX), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), UV-vis spectroscopy and Fourier-Transform infrared (FTIR) spectroscopy. The electrochemical performances were measured by using cyclic voltammetry and the result shows that after sintering the performance are significantly improved up to similar to 0.079 mA g(-1). We hope, our approach will opens up a new opportunity for such materials in energy storage devices.
资助项目Higher Education Commission of Pakistan
WOS关键词CATHODE MATERIAL ; LITHIUM ; GRAPHENE
WOS研究方向Materials Science
语种英语
出版者IOP PUBLISHING LTD
WOS记录号WOS:000466001000021
资助机构Higher Education Commission of Pakistan
内容类型期刊论文
源URL[http://ir.ipe.ac.cn/handle/122111/28148]  
专题中国科学院过程工程研究所
通讯作者Ullah, Hameed; Thebo, Khalid Hussain
作者单位1.Hazara Univ Mansehra, Dept Chem, Khyber Pakhtunkhwa 21300, Pakistan
2.Univ Peshawar, Islamia Coll, Dept Chem, Khyber Pakhtunkhwa, Pakistan
3.Kohat Univ Sci & Technol, Dept Phys, Kohat 26000, Khyber Pakhtunk, Pakistan
4.Shah Abdul Latif Univ KhairPur Mirs, Inst Chem, Sindh 66020, Pakistan
5.Chinese Acad Sci, Inst Proc Engn, CAS State Key Lab Multiphase Complex Syst, Beijing 100190, Peoples R China
6.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
7.Shenzhen Univ, Coll Elect Sci & Technol, Shenzhen 518060, Peoples R China
8.Shenzhen Univ, THz Tech Res Ctr, Shenzhen 518060, Peoples R China
推荐引用方式
GB/T 7714
Khan, Jamshid,Ullah, Hameed,Sajjad, Muhammad,et al. Controlled synthesis of ammonium manganese tri-fluoride nanoparticles with enhanced electrochemical performance[J]. MATERIALS RESEARCH EXPRESS,2019,6(7):11.
APA Khan, Jamshid.,Ullah, Hameed.,Sajjad, Muhammad.,Jatoi, Wahid Bux.,Ali, Akbar.,...&Thebo, Khalid Hussain.(2019).Controlled synthesis of ammonium manganese tri-fluoride nanoparticles with enhanced electrochemical performance.MATERIALS RESEARCH EXPRESS,6(7),11.
MLA Khan, Jamshid,et al."Controlled synthesis of ammonium manganese tri-fluoride nanoparticles with enhanced electrochemical performance".MATERIALS RESEARCH EXPRESS 6.7(2019):11.
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