Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase

	Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase
	Zhou, LM ; Liu, XL ; Li, ZS ; Wang, QH ; Zhu, DQ ; Hu, DH
刊名	CHINESE JOURNAL OF CHEMISTRY
	1996
卷号	14 期号:4 页码:348-353
关键词	Modified Cyclodextrin Enantiomeric Separation Alpha-phenylethylamine And Its Analogs
ISSN号	1001-604X
文献子类	Article
英文摘要	A mixed stationary phase of modified beta-cyclodextrin, 2,6-di-O-butyl-3-O-butyryl-beta-cyclodextrin (phase A), and SE-54 (phase B) was used for enantiomeric separation of alpha-phenylethylamine, o,m,p-methyl and o,m,p-methoxy-substituted analogs. The composition of mixed phase was selected by comparison of each calculated alpha(min)(=(gamma(m,i+1))/(gamma(m,i))), the relative retention values of the most adjacent peaks, and gamma(m,last), the relative retention values of the last eluting peak at each preselected ratio. Values of gamma(m,i), alpha calculated by derived equations were in good agreement with the experimental results obtained with two specified mixed phases. All solutes investigated a ere almost baseline separated at a predicted composition of phase A and phase B in a single run within 18 minutes.
WOS关键词	GAS-CHROMATOGRAPHY
WOS研究方向	Chemistry
语种	英语
出版者	SCIENCE CHINA PRESS
WOS记录号	WOS:A1996VQ56100010
内容类型	期刊论文
源URL	[http://cas-ir.dicp.ac.cn/handle/321008/168028]
专题	大连化学物理研究所_中国科学院大连化学物理研究所
作者单位	1.CHINESE ACAD SCI,DALIAN INST CHEM PHYS,DALIAN 116012,LIAONING,PEOPLES R CHINA 2.FUJIAN QUANZHOU TEACHERS COLL,DEPT CHEM,QUANZHOU 362000,FUJIAN,PEOPLES R CHINA
推荐引用方式 GB/T 7714	Zhou, LM,Liu, XL,Li, ZS,et al. Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase[J]. CHINESE JOURNAL OF CHEMISTRY,1996,14(4):348-353.
APA	Zhou, LM,Liu, XL,Li, ZS,Wang, QH,Zhu, DQ,&Hu, DH.(1996).Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase.CHINESE JOURNAL OF CHEMISTRY,14(4),348-353.
MLA	Zhou, LM,et al."Enantiomeric separation of alpha-phenylethylamine and its analogs by mixed chiral and achiral stationary phase".CHINESE JOURNAL OF CHEMISTRY 14.4(1996):348-353.