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	Synthesis of oxyresveratrol
	Sun Hongyi1,2,3; Xiao Chunfen1,2,3; Wei Wen1; Chen Yu1,2,3; Lue Zeliang1,2,3; Zou Yong1
刊名	Chinese journal of organic chemistry
	2010-10-01
卷号	30期号:10页码:1574-1579
关键词	Oxyresveratrol Phenylacetic acid Willgerodt-kindler rearrangement Methylation Perkin reaction Decarboxylation Demethylation
ISSN号	0253-2786
通讯作者	Sun hongyi()
英文摘要	A convenient method for the practical synthesis of oxyresveratrol is described. starting from the readily available 3,5-dihydroxyacetophenone (1), 3,5-dimethoxyphenylacetic acid (3) can be achieved through methylation and willgerodt-kindler rearrangement. perkin condensation between 3 and 2,4-dimethoxybenzaldehyde (4) formed the stilbene skeleton, and by subsequent decarboxylation and demethylation/isomerization process, oxyresveratrol (7) was obtained in an overall yield of 30%. the synthetic method has several advantages such as mild reaction conditions, high yield of product and simple operations. the structures of the target compound and key intermediates were verified by ms, ir, (1)h nmr and (13)c nmr techniques.
WOS关键词	RESVERATROL ; CELLS ; CIS
WOS研究方向	Chemistry
WOS类目	Chemistry, Organic
语种	英语
出版者	SCIENCE CHINA PRESS
WOS记录号	WOS:000283962200023
内容类型	期刊论文
URI标识	http://www.corc.org.cn/handle/1471x/2411168
专题	中国科学院大学
通讯作者	Sun Hongyi
作者单位	1.Chinese Acad Sci, Guangzhou Inst Chem, Guangzhou 510650, Guangdong, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China 3.Qujing Normal Univ, Dept Chem & Chem Engn, Qujing 655011, Peoples R China
推荐引用方式 GB/T 7714	Sun Hongyi,Xiao Chunfen,Wei Wen,et al. Synthesis of oxyresveratrol[J]. Chinese journal of organic chemistry,2010,30(10):1574-1579.
APA	Sun Hongyi,Xiao Chunfen,Wei Wen,Chen Yu,Lue Zeliang,&Zou Yong.(2010).Synthesis of oxyresveratrol.Chinese journal of organic chemistry,30(10),1574-1579.
MLA	Sun Hongyi,et al."Synthesis of oxyresveratrol".Chinese journal of organic chemistry 30.10(2010):1574-1579.

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