Synthesis and photocatalytic activity of highly dispersed tio2/sba-15 | |
Zhang Shu-Cui1,2; Jiang Dong1; Tang Tao1,2; Li Jun-Hua1,2; Xu Yao1 | |
刊名 | Acta physico-chimica sinica |
2010-05-01 | |
卷号 | 26期号:5页码:1330-1336 |
关键词 | Photocatalysis Carboxylate-modified Tio2 Sba-15 Solvothermal |
ISSN号 | 1000-6818 |
DOI | 10.3866/pku.whxb20100520 |
通讯作者 | Jiang dong(jdred@sxicc.ac.cn) |
英文摘要 | Highly dispersed tio2/sba-15 photocatalysts were successfully synthesized by solvothermal treatment using titanium n-butoxide (tb) and carboxylate. modified sba-15 (cooh/sba-15) as raw materials. the good dispersive carboxyl groups of cooh/sba-15 coordinated with tb molecules to anchor them. after solvothermal treatment, the tb molecules were transformed into tio2 nanoparticles and finally formed the tio2/sba-15 products. the products were calcined to improve the crystallization of tio2 and to remove the organic compounds. as. obtained tio2/sba-15 photocatalysts were characterized by x. ray diffraction (xrd), nitrogen adsorption, fourier transform infrared (fi-ir) spectroscopy, and transmission electron microscopy (tem). analytical results showed that the as. obtained tio2/sba-15 photocatalysts possessed a better mesoporous structure and a larger specific surface area. the highly crystalline anatase tio2 nanocrystals dispersed well on the surface of sba-15. rhodamine b (rhb), as a photodegradation target, was used to evaluate photocatalytic performance under uv light irradiation. the as. obtained tio2/sba-15 photocatalysts exhibited much better photocatalytic activity compared with the photocatalysts prepared by a post. synthesis impregnation method. |
WOS关键词 | SUPPORTED TIO2 PHOTOCATALYSTS ; MESOPOROUS SILICA ; RAMAN-SPECTRUM ; ANATASE TIO2 ; TITANIA ; NANOPARTICLES ; SBA-15 ; DEGRADATION ; ADSORPTION ; FILMS |
WOS研究方向 | Chemistry |
WOS类目 | Chemistry, Physical |
语种 | 英语 |
出版者 | PEKING UNIV PRESS |
WOS记录号 | WOS:000277881600024 |
内容类型 | 期刊论文 |
URI标识 | http://www.corc.org.cn/handle/1471x/2409955 |
专题 | 中国科学院大学 |
通讯作者 | Jiang Dong |
作者单位 | 1.Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan 030001, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Zhang Shu-Cui,Jiang Dong,Tang Tao,et al. Synthesis and photocatalytic activity of highly dispersed tio2/sba-15[J]. Acta physico-chimica sinica,2010,26(5):1330-1336. |
APA | Zhang Shu-Cui,Jiang Dong,Tang Tao,Li Jun-Hua,&Xu Yao.(2010).Synthesis and photocatalytic activity of highly dispersed tio2/sba-15.Acta physico-chimica sinica,26(5),1330-1336. |
MLA | Zhang Shu-Cui,et al."Synthesis and photocatalytic activity of highly dispersed tio2/sba-15".Acta physico-chimica sinica 26.5(2010):1330-1336. |
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