Preparation and characterization of core-shell structured alpha-fe2o3/sic spheres | |
Wu, Xiangyang; Jin, Guoqiang; Guan, Lianxiu; Cao, Hu; Guo, Xiang-Yun | |
刊名 | Materials science and engineering a-structural materials properties microstructure and processing |
2006-10-15 | |
卷号 | 433期号:1-2页码:190-194 |
关键词 | Silicon carbide Iron oxide Core-shell structure Magnetic properties |
ISSN号 | 0921-5093 |
DOI | 10.1016/j.msea.2006.07.013 |
通讯作者 | Guo, xiang-yun(xyguo@sxicc.ac.cn) |
英文摘要 | Fe2o3/sic composite microspheres with a core-shell structure were prepared by the carbothermal reduction reaction between poly(styrene sulfonic acid) iron salt and silica. x-ray diffraction, scanning electron microscope and magnetic properties measurement system were employed to characterize the morphology, structure and magnetic properties of the microspheres. from the results, the microspheres with a diameter of 150-400 mu m have an alpha-fe2o3 core and a sic shell of tens of microns in thickness. the magnetism of the core-shell structured spheres at 10(4) oe is much larger than that of pure alpha-fe2o3 spheres prepared under the same conditions and the increment in magnetism is attributed to the introduction of iron silicides and sic. by further chemical treatment, the alpha-fe2o3/sic microspheres can change into sic hollow spheres, which have diameters similar to the magnetic spheres and mainly consist of irregular sic particles. the formation mechanism of the composite and hollow spheres was also discussed. (c) 2006 elsevier b.v. all rights reserved. |
WOS关键词 | REACTIVE REPLICA TECHNIQUE ; TUBULAR SILICON-CARBIDE ; ION-EXCHANGE-RESIN ; MESOPOROUS SILICA ; CARBON ; PARTICLES ; NANOWIRES ; NANOPARTICLES ; TEMPLATES ; NANOTUBES |
WOS研究方向 | Science & Technology - Other Topics ; Materials Science ; Metallurgy & Metallurgical Engineering |
WOS类目 | Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering |
语种 | 英语 |
出版者 | ELSEVIER SCIENCE SA |
WOS记录号 | WOS:000240821400029 |
内容类型 | 期刊论文 |
URI标识 | http://www.corc.org.cn/handle/1471x/2379842 |
专题 | 中国科学院大学 |
通讯作者 | Guo, Xiang-Yun |
作者单位 | 1.CAS, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan 030001, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Wu, Xiangyang,Jin, Guoqiang,Guan, Lianxiu,et al. Preparation and characterization of core-shell structured alpha-fe2o3/sic spheres[J]. Materials science and engineering a-structural materials properties microstructure and processing,2006,433(1-2):190-194. |
APA | Wu, Xiangyang,Jin, Guoqiang,Guan, Lianxiu,Cao, Hu,&Guo, Xiang-Yun.(2006).Preparation and characterization of core-shell structured alpha-fe2o3/sic spheres.Materials science and engineering a-structural materials properties microstructure and processing,433(1-2),190-194. |
MLA | Wu, Xiangyang,et al."Preparation and characterization of core-shell structured alpha-fe2o3/sic spheres".Materials science and engineering a-structural materials properties microstructure and processing 433.1-2(2006):190-194. |
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