Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry | |
Pang, Tao; Yuan, Zhongyi; Dai, Yongsheng; Wang, Chang; Yang, Jun; Peng, Liming; Xu, Guowang | |
刊名 | journal of separation science |
2007-02-01 | |
卷号 | 30期号:3页码:289-296 |
关键词 | APCI glycosides MS tobacco |
通讯作者 | 许国旺 |
产权排序 | 1;1 |
英文摘要 | hplc-atmospheric pressure chemical ionization ms (hplc-apci-ms) was used to screen and identify glycosides in tobacco leaf. ms/ms and ms3 and photodiode array (pda) detection were also used in the characterization. a total of 12 glycosides were found and four of them were identified based on their abundant [m + h](+) ions, uv and ms/ms analysis and they are scopolin, rutin, quercetin-3-glycoside, and spectra, kaempferol-3-rutino side. analytical characteristics of the method were investigated. the contents of these glycosides were obtained and compared based on the relative peak area to the internal standard in seven kinds of tobacco leaf. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | flavonoid glycosides ; xanthone glycosides ; urine samples ; aglycones ; quantification ; ms |
收录类别 | SCI |
原文出处 | true |
语种 | 英语 |
WOS记录号 | WOS:000244768400001 |
公开日期 | 2010-11-30 |
内容类型 | 期刊论文 |
源URL | [http://159.226.238.44/handle/321008/98795] |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&D Ctr, Dalian 116023, Peoples R China 2.Chinese Acad Sci, Shanghai Inst Biol Sci, Inst Biochem & Cell Biol, Shanghai, Peoples R China 3.Chuxiong Cigarette Co, Hongta Grp, Chuxiong, Yunnan, Peoples R China |
推荐引用方式 GB/T 7714 | Pang, Tao,Yuan, Zhongyi,Dai, Yongsheng,et al. Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry[J]. journal of separation science,2007,30(3):289-296. |
APA | Pang, Tao.,Yuan, Zhongyi.,Dai, Yongsheng.,Wang, Chang.,Yang, Jun.,...&Xu, Guowang.(2007).Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry.journal of separation science,30(3),289-296. |
MLA | Pang, Tao,et al."Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry".journal of separation science 30.3(2007):289-296. |
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