Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry
Pang, Tao; Yuan, Zhongyi; Dai, Yongsheng; Wang, Chang; Yang, Jun; Peng, Liming; Xu, Guowang
刊名journal of separation science
2007-02-01
卷号30期号:3页码:289-296
关键词APCI glycosides MS tobacco
通讯作者许国旺
产权排序1;1
英文摘要hplc-atmospheric pressure chemical ionization ms (hplc-apci-ms) was used to screen and identify glycosides in tobacco leaf. ms/ms and ms3 and photodiode array (pda) detection were also used in the characterization. a total of 12 glycosides were found and four of them were identified based on their abundant [m + h](+) ions, uv and ms/ms analysis and they are scopolin, rutin, quercetin-3-glycoside, and spectra, kaempferol-3-rutino side. analytical characteristics of the method were investigated. the contents of these glycosides were obtained and compared based on the relative peak area to the internal standard in seven kinds of tobacco leaf.
WOS标题词science & technology ; physical sciences
类目[WOS]chemistry, analytical
研究领域[WOS]chemistry
关键词[WOS]flavonoid glycosides ; xanthone glycosides ; urine samples ; aglycones ; quantification ; ms
收录类别SCI
原文出处true
语种英语
WOS记录号WOS:000244768400001
公开日期2010-11-30
内容类型期刊论文
源URL[http://159.226.238.44/handle/321008/98795]  
专题大连化学物理研究所_中国科学院大连化学物理研究所
作者单位1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&D Ctr, Dalian 116023, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Biol Sci, Inst Biochem & Cell Biol, Shanghai, Peoples R China
3.Chuxiong Cigarette Co, Hongta Grp, Chuxiong, Yunnan, Peoples R China
推荐引用方式
GB/T 7714
Pang, Tao,Yuan, Zhongyi,Dai, Yongsheng,et al. Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry[J]. journal of separation science,2007,30(3):289-296.
APA Pang, Tao.,Yuan, Zhongyi.,Dai, Yongsheng.,Wang, Chang.,Yang, Jun.,...&Xu, Guowang.(2007).Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry.journal of separation science,30(3),289-296.
MLA Pang, Tao,et al."Identification and determination of glycosides in tobacco leaves by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry".journal of separation science 30.3(2007):289-296.
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