On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum

	On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum
	Zhang, Jie ; Zhang, Lihua ; Duan, Jicheng ; Liang, Zhen ; Zhang, Weibing ; Hu, Yushu ; Zhang, Yukui
刊名	journal of separation science
	2006-11-01
卷号	29 期号:16 页码:2514-2522
关键词	Ganoderma lucidum mass spectrometry natural products supercritical fluid extraction
通讯作者	张丽华
产权排序	1;1
英文摘要	a novel on-line system combining supercritical fluid extraction (sfe) and two-dimensional high performance liquid chromatography (2d-hplc) was developed. a trap column and two three-port valves were employed to couple sfe and 2d-hplc system, which was composed of a cn column and a monolithic silica column, connected by a 10-port dual-position valve. the analytes extracted by supercritical co2 were completely transferred to the 2d-hplc system. after separation in two orthogonal modes, the eluents were delivered to apci-tandem-ms for identification of the samples. in this way, sample preparation, separation, detection, and identification were integrated into an on-line system permitting analysis of the fruiting bodies of ganoderma lucidum, and at least 73 components in the extract were resolved with calculated peak capacity of up to 1643.
WOS标题词	science & technology ; physical sciences
类目[WOS]	chemistry, analytical
研究领域[WOS]	chemistry
关键词[WOS]	aromatic-hydrocarbons ; quantitative-analysis ; hplc system ; separation ; matrices ; triacylglycerols ; products ; column
收录类别	SCI
原文出处	true
语种	英语
WOS记录号	WOS:000242242300013
公开日期	2010-11-30
内容类型	期刊论文
源URL	[http://159.226.238.44/handle/321008/97575]
专题	大连化学物理研究所_中国科学院大连化学物理研究所
作者单位	1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian, Peoples R China 2.Univ Texas, Hlth Sci Ctr, San Antonio, TX 78285 USA
推荐引用方式 GB/T 7714	Zhang, Jie,Zhang, Lihua,Duan, Jicheng,et al. On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum[J]. journal of separation science,2006,29(16):2514-2522.
APA	Zhang, Jie.,Zhang, Lihua.,Duan, Jicheng.,Liang, Zhen.,Zhang, Weibing.,...&Zhang, Yukui.(2006).On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum.journal of separation science,29(16),2514-2522.
MLA	Zhang, Jie,et al."On-line hyphenation of supercritical fluid extraction and two-dimensional high performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometer for the analysis of Ganoderma lucidum".journal of separation science 29.16(2006):2514-2522.