| 题名 | 多孔整体材料新型吸附剂的制备及其应用研究; Study on the Preparation of Novel Sorbents based Porous Monolithic Materials and Its Application |
| 作者 | 张咏 |
| 答辩日期 | 2017-03-24 ; 2015-05-14 |
| 导师 | 黄晓佳 |
| 关键词 | 整体材料 搅拌饼固相萃取 整体材料纤维固相微萃取 聚离子液体 聚(乙二醇二甲基丙烯酸酯/氧化石墨烯) 聚(3-丙烯酰胺苯硼酸/二乙烯基苯) 聚(溴化-3-(1-乙基咪唑)丙基甲基丙烯酰氧胺/乙二醇二甲基丙烯酸酯) 聚(乙烯基咪唑/乙二醇二甲基丙烯酸酯) monolithic materials stir cake sorptive extraction monolithic fiber based solid phase microextraction polymeric ionic liquid poly(ethylene glycol dimethacrylate/graphene oxide) poly(3-acrylamidophenylboronic/divinylbenzene poly(3-(1-ethyl imidazolium-3-yl) popylmethacrylamido bormide/ethylene glycol dimethacrylate) poly(1-vinylimidazole/ethylene glycol dimethacrylate) |
| 英文摘要 | 整体材料因其制备简单、可“原位”聚合、通透性好、传质速率快、易化学改性等优点而被广泛应用于样品前处理过程中。本研究制备了四种新型整体材料，并结合搅拌饼固相萃取和纤维固相微萃取技术与高灵敏分析仪器联用，建立了环境水样中苯胺类、苯甲酰脲类农药、重金属锑和氯代酚类的分析方法。具体研究内容如下： 1.制备了掺杂氧化石墨烯的聚乙二醇二甲基丙烯酸酯整体材料(EDMA/GO)，并将其用作搅拌饼固相萃取(stircakesorptiveextraction,SCSE)的吸附剂，考察了不同单体、交联剂、致孔剂比例下制备的整体材料对苯胺类化合物萃取性能的影响，利用红外光谱、扫描电镜、透射电镜和元素分析等手段，对...; Monolithic materials were widely applied in the field of sample pretreatment due to the advantages such as facile preparation, good permeability, fast mass transport, ease of chemical modification. In present study, four novel porous monoliths were prepared and acted as extractive medium of stir cake sorptive extraction (SCSE) and monolithic fiber-based solid phase microextraction (MF-SPME). Simpl...; 学位：理学硕士; 院系专业：环境与生态学院_环境科学; 学号：33120121151661 |
| 语种 | zh_CN |
| 出处 | http://210.34.4.13:8080/lunwen/detail.asp?serial=50579 |
| 内容类型 | 学位论文 |
| 源URL | [http://dspace.xmu.edu.cn/handle/2288/130349]  |
| 专题 | 环境生态－学位论文 |
| 推荐引用方式 GB/T 7714 | 张咏. 多孔整体材料新型吸附剂的制备及其应用研究, Study on the Preparation of Novel Sorbents based Porous Monolithic Materials and Its Application[D]. 2017, 2015. |
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