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硫酸钾熔盐法微硅粉制备莫来石晶须研究
王涛 ; 铁生年 ; 汪长安 ; WANG Tao ; TIE Sheng-nian ; WANG Chang-an
2016-03-30 ; 2016-03-30
关键词微硅粉 熔盐 莫来石晶须 micro silica fume molten salt mullite whisker TQ175.1
其他题名Study on Preparation of Mullite Whisker by Molten Method Utilizing Micro Silica Fume
中文摘要以微硅粉和Al2(SO4)3为反应物料,硫酸钾为熔盐介质,分别在800℃、900℃、1000℃和1100℃下煅烧并保温1 h,溶解、过滤、烘干后得到白色疏松状莫来石粉体。利用XRD和SEM对合成粉体进行物相分析和显微形貌观察。结果表明:1000℃为合成莫来石最佳温度,合成的莫来石晶须直径为0.1~0.8μm,长度为4~5μm。同时对莫来石晶须的形成机理进行了探讨。; The mullite powders were prepared through reaction of micro silica fume and aluminum sulfate in molten potassium sulfate at different temperature of 800 ℃,900 ℃,1000 ℃ and 1100 ℃ for 1 h, sequently dissolved,separated and dried. The phase composition and morphology of synthesized powders were characterized by X-ray diffraction and scanning electron-microscopy. The results show that 1000 ℃ is regarded as the best synthesis temperature,and the mullite whiskers are 0. 1-0. 8 μm in diameter and 4-5 μm in length. Meanwhile,the formation mechanism of the mullite whiskers was discussed.
语种中文 ; 中文
内容类型期刊论文
源URL[http://ir.lib.tsinghua.edu.cn/ir/item.do?handle=123456789/141673]  
专题清华大学
推荐引用方式
GB/T 7714
王涛,铁生年,汪长安,等. 硫酸钾熔盐法微硅粉制备莫来石晶须研究[J],2016, 2016.
APA 王涛,铁生年,汪长安,WANG Tao,TIE Sheng-nian,&WANG Chang-an.(2016).硫酸钾熔盐法微硅粉制备莫来石晶须研究..
MLA 王涛,et al."硫酸钾熔盐法微硅粉制备莫来石晶须研究".(2016).
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