Preparation and characterization of Antheraea pernyi silk fibroin based nanohydroxyapatite composites | |
Ren, Y. J. ; Sun, X. D. ; Cui, F. Z. ; Wei, Y. T. ; Cheng, Z. J. ; Kong, X. D. | |
2010-05-10 ; 2010-05-10 | |
关键词 | antheraea pernyi silk fibroin hydroxyapatite nanocomposite OSTEOBLAST ADHESION NANOPHASE CERAMICS HYDROXYAPATITE NANOCRYSTALS CONFORMATIONAL-CHANGES MINERALIZED COLLAGEN BONE FILMS PEPTIDES SCAFFOLD NANOCOMPOSITES Biotechnology & Applied Microbiology Materials Science, Biomaterials Polymer Science |
中文摘要 | In the present study, Antheraea pernyi silk fibroin (Ap-SF) is employed to regulate the mineralization of hydroxyapatite (HAp) nanocrystals. Calcium phosphate crystals precipitate in the aqueous solution of regenerated Ap-SF at pH 7.4 and room temperature. The samples are charaterized with X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and scanning electron microscopy (SEM). Based on the XRD results, the inorganic phase in the mineralized Ap-SF composites is HAp as small particles with low crystallinity. The FTIR analysis reveals that the HAp crystals are carbonate-substituted HAp and compounded with Ap-SF. The TEM images show mineralized nanofibrils in the composites as rod-like shapes 4-5mn in diameter. Electron diffraction (SAED) patterns of selected areas of the composites exhibit polycrystalline rings that are ascribed to HAp. SEM images show mineralized Ap-SF composites with several mineralized rods 49-74nm in diameter. |
语种 | 英语 ; 英语 |
出版者 | SAGE PUBLICATIONS LTD ; LONDON ; 1 OLIVERS YARD, 55 CITY ROAD, LONDON EC1Y 1SP, ENGLAND |
内容类型 | 期刊论文 |
源URL | [http://hdl.handle.net/123456789/21026] |
专题 | 清华大学 |
推荐引用方式 GB/T 7714 | Ren, Y. J.,Sun, X. D.,Cui, F. Z.,et al. Preparation and characterization of Antheraea pernyi silk fibroin based nanohydroxyapatite composites[J],2010, 2010. |
APA | Ren, Y. J.,Sun, X. D.,Cui, F. Z.,Wei, Y. T.,Cheng, Z. J.,&Kong, X. D..(2010).Preparation and characterization of Antheraea pernyi silk fibroin based nanohydroxyapatite composites.. |
MLA | Ren, Y. J.,et al."Preparation and characterization of Antheraea pernyi silk fibroin based nanohydroxyapatite composites".(2010). |
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