Magnetic retrieval of chitosan: Extraction of bioactive constituents from green tea beverage samples
Zhang HF(张洪飞)1,2; Shi YP(师彦平)1
刊名Analyst
2012
卷号137期号:4页码:910-916
ISSN号0003-2654
通讯作者师彦平
英文摘要

A new solid-phase extraction mode for magnetic retrieval of chitosan combined with high-performance liquid chromatography-diode array detection was proposed for the pre-concentration and determination of flavonoids in green tea beverage samples. In the experiment, chitosan was used as sorbents for the extraction of target analytes; after completion of the extraction process, Fe3O4 nanoparticles acted as carrier to retrieve chitosan from the sample solution. Some important parameters influenced extraction efficiency of flavonoids, including the extraction mode, amounts of chitosan, pH of sample solution, extraction time, salt addition, amounts of Fe3O4 nanoparticles, desorption solvent and desroption time, were optimized. Under the optimum conditions, the recoveries of analytes done on samples spiked with the target analytes were between 96.4% and 108.6%; relative standard deviations ranged from 0.6% to 8.7%. The correlation coefficients varied from 0.9917 to 0.9988. The limits of detection ranged from 5.4 to 16.8 ng mL−1 at a signal-to-noise ratio of 3. All four different brands of green tea beverage samples were successfully analyzed by the proposed method.

学科主题分析化学与药物化学
收录类别SCI
资助信息the National Natural Science Foundation of China (No. 21075127;20875095)
语种英语
WOS记录号WOS:000299476300018
公开日期2016-05-03
内容类型期刊论文
源URL[http://210.77.64.217/handle/362003/19507]  
专题兰州化学物理研究所_中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室
作者单位1.Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, P. R. China
2.Graduate University of Chinese Academy of Sciences, Beijing, P. R. China
推荐引用方式
GB/T 7714
Zhang HF,Shi YP. Magnetic retrieval of chitosan: Extraction of bioactive constituents from green tea beverage samples[J]. Analyst,2012,137(4):910-916.
APA Zhang HF,&Shi YP.(2012).Magnetic retrieval of chitosan: Extraction of bioactive constituents from green tea beverage samples.Analyst,137(4),910-916.
MLA Zhang HF,et al."Magnetic retrieval of chitosan: Extraction of bioactive constituents from green tea beverage samples".Analyst 137.4(2012):910-916.
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